Please use this identifier to cite or link to this item: https://idr.l3.nitk.ac.in/jspui/handle/123456789/10299
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dc.contributor.authorShetty, A.Nityananda
dc.contributor.authorGadag, R.V.
dc.contributor.authorGajendragad, M.R.
dc.date.accessioned2020-03-31T08:18:53Z-
dc.date.available2020-03-31T08:18:53Z-
dc.date.issued1989
dc.identifier.citationIndian Journal of Technology, 1989, Vol.27, 4, pp.224-226en_US
dc.identifier.urihttp://idr.nitk.ac.in/jspui/handle/123456789/10299-
dc.description.abstractA method is proposed for selective complexometric determination of Pd(II) using hydroxylamine hydrochloride as a replacing (masking) agent. An excess of EDTA is added to Pd(II) solution containing associated diverse metal ions and the uncomplexed EDTA is titrated at pH 5-6 (acetic acid - acetate buffer) with lead nitrate solution using xylenol orange as indicator. Hydroxylamine hydrochloride is then added to displace EDTA from the Pd-EDTA complex. The released EDTA is titrated with standard lead nitrate solution. Reproducible and accurate results are obtained in the concentration range 0.3-15 mg of Pd with a relative error of 0.4% and coefficient of variation (n=6) not exceeding 0.4%.en_US
dc.titleComplexometric determination of palladium (II) using hydroxylamine hydrochloride as releasing agenten_US
dc.typeArticleen_US
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